Scheda di dettaglio – i prodotti della ricerca
| Dato | Valore |
|---|---|
| Title | RECOVERY OF 4-NONYLPHENOL AND 4-NONYLPHENOL ETHOXYLATES FROM RIVER SEDIMENTS BY PRESSURISED LIQUID EXTRACTION |
| Abstract | The pressurised liquid extraction (PLE) of 4-nonylphenol (4-NP) with methanol (1008C and 100 atm) from river sediments was compared with methanolic Soxhlet extraction, the standard method for the sediment analysis. The PLE method showed a precision (average RSD ranged from 6 to 33%) and an accuracy (average recovery 85 and 87% for 4-NP and 4-NPE, respectively) comparable to those of Soxhlet. The extraction was performed on river sediments and no organic carbon content influence was found. The comparative study presented in this paper demonstrates that PLE is an alternative suitable extraction method for 4-nonylphenol and 4-nonylphenol ethoxylate determination in sediments. |
| Source | Journal of chromatography (Print) 325, pp. 297–301 |
| Keywords | Pressurised liquid extraction4-Nonylphenol4-Nonylphenol ethoxylate |
| Journal | Journal of chromatography (Print) |
| Editor | Elsevier, Amsterdam, Paesi Bassi |
| Year | 2001 |
| Type | Articolo in rivista |
| Authors | VALSECCHI S., POLESELLO S., CAVALLI S. |
| Text | 42334 2001 Pressurised liquid extraction 4 Nonylphenol 4 Nonylphenol ethoxylate RECOVERY OF 4 NONYLPHENOL AND 4 NONYLPHENOL ETHOXYLATES FROM RIVER SEDIMENTS BY PRESSURISED LIQUID EXTRACTION VALSECCHI S., POLESELLO S., CAVALLI S. CNR IRSA, via Mornera 25, I 20047 Brugherio, Italy Dionex, via Tulipani 5, I 20090 Pieve Emanuele, Italy The pressurised liquid extraction PLE of 4 nonylphenol 4 NP with methanol 1008C and 100 atm from river sediments was compared with methanolic Soxhlet extraction, the standard method for the sediment analysis. The PLE method showed a precision average RSD ranged from 6 to 33% and an accuracy average recovery 85 and 87% for 4 NP and 4 NPE, respectively comparable to those of Soxhlet. The extraction was performed on river sediments and no organic carbon content influence was found. The comparative study presented in this paper demonstrates that PLE is an alternative suitable extraction method for 4 nonylphenol and 4 nonylphenol ethoxylate determination in sediments. 325 RECOVERY OF 4 NONYLPHENOL AND 4 NONYLPHENOL ETHOXYLATES FROM RIVER SEDIMENTS BY PRESSURISED LIQUID EXTRACTION NP_ASE.pdf Articolo in rivista Elsevier 0021 9673 Journal of chromatography Print Journal of chromatography Print J. chromatogr. Print Journal of chromatography. Print Journal of chromatography. A Print stefano.polesello POLESELLO STEFANO saramaria.valsecchi VALSECCHI SARA MARIA |