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DatoValore
TitleCalibration of a new device to measure water content of rocks.
AbstractLarge-scale problems of water quality and water availability require knowledge of water travel times through the unsaturated zone and substances carried with it. A number of methods and devices are available for measuring the water content in soils but usually they are not usable with the rocks too and very few are the attempts to verify their applicability. In applying the devices for water content estimation in rocks, the main difficulty is related to the installation of the probes. The installation procedure have to ensure a good contact between the rock and the sensor in order to reduce the uncertainty due to the gap effects. In this study a non-traditional method, known as electrical impedance spectrometry (EIS), was used. Using the new apparatus Z-meter, the electrical impedance in complex form and its changes were monitored in order to verify the suitability of the device with the rock. One kind of stainless steel probes have been installed into samples of calcarenite, a sedimentary rock coming from a quarry located in Canosa (South of Italy). The relationship between water content and resistance and between the reactance and the rock characteristics, such as texture, structure, etc., were investigated within a frequency range from 100Hz to 10000Hz, by using water with different electrical conductivity (EC) values. The experimentation was performed in environment with controlled temperature, due to the influence of temperature variation on all indirect moisture measurement methods. The experimental tests have been performed three times using exactly the same experimental set up, in order to check the repeatability of the data. The results allowed to define the calibration curves at different EC values for the calcarenite. This represent an important result because defines the possibility of using a new device, the Z-meter, to measure the rock water content by overcoming the issue of the gap effect that causes uncertainty of the measured values. This opens new scenarios linked to the possibility to monitor in situ flow and transport processes, that occur in the vadose zone constituted from rocks, measures rarely performed until now.
Source3rd Conference and Working Session Within the frame of the International Program EUREKA Project No.: E!4981, Brno, CZ, September 20-21 2012
KeywordsRock water contentcalibrationelectrical impedance spectrometry.
Year2012
TypeContributo in atti di convegno
AuthorsCaputo M.C., Masciale R.
Text323066 2012 Rock water content calibration electrical impedance spectrometry. Calibration of a new device to measure water content of rocks. Caputo M.C., Masciale R. CNR IRSA UOS Bari Large scale problems of water quality and water availability require knowledge of water travel times through the unsaturated zone and substances carried with it. A number of methods and devices are available for measuring the water content in soils but usually they are not usable with the rocks too and very few are the attempts to verify their applicability. In applying the devices for water content estimation in rocks, the main difficulty is related to the installation of the probes. The installation procedure have to ensure a good contact between the rock and the sensor in order to reduce the uncertainty due to the gap effects. In this study a non traditional method, known as electrical impedance spectrometry EIS , was used. Using the new apparatus Z meter, the electrical impedance in complex form and its changes were monitored in order to verify the suitability of the device with the rock. One kind of stainless steel probes have been installed into samples of calcarenite, a sedimentary rock coming from a quarry located in Canosa South of Italy . The relationship between water content and resistance and between the reactance and the rock characteristics, such as texture, structure, etc., were investigated within a frequency range from 100Hz to 10000Hz, by using water with different electrical conductivity EC values. The experimentation was performed in environment with controlled temperature, due to the influence of temperature variation on all indirect moisture measurement methods. The experimental tests have been performed three times using exactly the same experimental set up, in order to check the repeatability of the data. The results allowed to define the calibration curves at different EC values for the calcarenite. This represent an important result because defines the possibility of using a new device, the Z meter, to measure the rock water content by overcoming the issue of the gap effect that causes uncertainty of the measured values. This opens new scenarios linked to the possibility to monitor in situ flow and transport processes, that occur in the vadose zone constituted from rocks, measures rarely performed until now. Eureka 2012 Proceedings of 3rd Conference and Working Session Within the frame of the International Program EUREKA Project No. E 4981 9788021445376 3rd Conference and Working Session Within the frame of the International Program EUREKA Project No. E 4981 Brno, CZ September 20 21 2012 Internazionale Contributo Contributo in atti di convegno mariaclementina.caputo CAPUTO MARIA CLEMENTINA rita.masciale MASCIALE RITA